Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Bromophenethylamine → 4'-(2-Aminoethyl)-3-biphenylcarboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Bromophenethylamine | HCID 533915 | — |
| 반응물 | (3-Carbamoylphenyl)boronic acid | HCID 2737814 | — |
| 반응물 | Toluene ethanol | HCID 21863594 | — |
| 용매 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 생성물 | 4'-(2-Aminoethyl)-3-biphenylcarboxamide | HCID 58276405 | — |
반응 단계
The title compound was prepared from 3-(aminocarbonyl)-phenyl boronic acid and 4-bromophenethylamine according to the procedure described for intermediate I-VII-1 with the exceptions that 4:1 PhMe/EtOH was sued as organic solvent (instead of DME) and the chromatographic purification step was omitted. LC/MS (method E) 0.53 min; m/z 241 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08822518B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-d3081091b1fe44fa8a47eb45f5cae40c |
| 출처 메모 | uspto-grants-2014_09 |