Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzenesulfonyl chloride, 3,4-dichloro- → 3,4-dichloro-N-[5-chloro-2-(methylthio)phenyl]benzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzenesulfonyl chloride, 3,4-dichloro- | HCID 7383 | — |
| 반응물 | 5-Chloro-2-(methylsulfinyl)aniline | HCID 67972850 | — |
| 생성물 | 3,4-dichloro-N-[5-chloro-2-(methylthio)phenyl]benzenesulfonamide | HCID 67972217 | 21.4% |
반응 단계
Following General Procedure B, the title compound (52 mg, 21%) was prepared from 5-chloro-2-(methylsulfinyl)aniline (Intermediate 2) (120 mg, 0.635 mmol) and 3,4-dichlorobenzene-1-sulfonyl chloride (156 mg, 0.635 mmol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08822530B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-a6728c0286504da2934217103634da1f |
| 출처 메모 | uspto-grants-2014_09 |