Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chloro-2-fluorobenzene-1-sulfonyl chloride → 4-chloro-N-[5-chloro-2-(methylthio)phenyl]-2-fluorobenzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chloro-2-fluorobenzene-1-sulfonyl chloride | HCID 2778860 | — |
| 반응물 | 5-Chloro-2-(methylthio)aniline | HCID 2794577 | — |
| 생성물 | 4-chloro-N-[5-chloro-2-(methylthio)phenyl]-2-fluorobenzenesulfonamide | HCID 57378996 | 66.1% |
반응 단계
Following General Procedure B, the title compound (380 mg, 66%) was prepared from 5-chloro-2-(methylthio)aniline (273 mg, 1.57 mmol) and 4-chloro-2-fluorobenzene-1-sulfonyl chloride (360 mg, 1.57 mmol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08822530B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-982143bef10140259238f754cc72e738 |
| 출처 메모 | uspto-grants-2014_09 |