Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 5-Fluoro-2-((3-nitrobenzyl)thio)aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Benzene, 1-(bromomethyl)-3-nitro- | HCID 77568 | — |
| 반응물 | 2-Amino-4-fluorobenzene-1-thiol | HCID 11105480 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 5-Fluoro-2-((3-nitrobenzyl)thio)aniline | HCID 43304416 | 97% |
반응 단계
Following General Procedure A, the title compound (460 mg, 97%) was prepared from 2-amino-4-fluorobenzenethiol (562 g, 3.93 mmol), 1-(bromomethyl)-3-nitrobenzene (566 mg, 2.62 mmol), K2CO3 (1.8 g, 13.10 mmol) in DMF (10 ml).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08822530B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-697136108b5845e3b32265b19abeb3d1 |
| 출처 메모 | uspto-grants-2014_09 |