참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,1-Dichlorosilacyclobutane | HCID 75373 | — |
| 반응물 | 2-Trimethylsilylacetate | HCID 22558220 | — |
| 생성물 | 1,1-Diacetoxysilacyclobutane | HCID 15065919 | — |
반응 단계
To 30.0 g trimethylsilylacetate was added 16.0 g 1,1-dichlorosilacyclobutane. The reactants were stirred for one hour at 25° C. and fractional distillation performed on the reaction mixture. The title compound was isolated as a clear, colorless fluid. The yield was 14.6 g (81.4%). The structure of the product was confirmed by mass spectroscopy and nuclear magnetic resonance spectroscopy (NMR).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04985565 |
|---|
| 출처 데이터셋 | uspto-grants-1991_01 |
|---|
| ORD ID | ord-bee8c52996154db1b1910529339899a1 |
|---|
| 출처 메모 | uspto-grants-1991_01 |
|---|
