Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-Trimethylsilyl-N-methylacetamide → 1-Methyl-1-(N-methylacetamido)silacyclobutane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-Trimethylsilyl-N-methylacetamide | HCID 81953 | — |
| 반응물 | Silacyclobutane, 1-chloro-1-methyl- | HCID 137554 | — |
| 생성물 | 1-Methyl-1-(N-methylacetamido)silacyclobutane | HCID 15065924 | — |
반응 단계
To 30.02 g 1-chloro-1-methylsilacyclobutane was added 36.10 g N-methyl-N-(trimethylsilyl)acetamide. The reaction products were fractionally distilled. The title compound was isolated as a clear, colorless fluid with a boiling point of 68°-76° C. at 3.6 mm Hg. The yield was 31.56 g (86%). The product was identified by NMR and mass spectroscopy.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04985565 |
| 출처 데이터셋 | uspto-grants-1991_01 |
| ORD ID | ord-b1a50ac77d5a4b2db5988d6d1a87bed9 |
| 출처 메모 | uspto-grants-1991_01 |