Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1-Dichlorosilacyclobutane → 1,1-Diacetamidosilacyclobutane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1-Dichlorosilacyclobutane | HCID 75373 | — |
| 반응물 | Acetamide, 2-(trimethylsilyl)- | HCID 357676 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 1,1-Diacetamidosilacyclobutane | HCID 20075523 | — |
반응 단계
When 1.72 g of trimethylsilylacetamide was mixed with 0.92 g of 1,1-dichlorosilacyclobutane in 5 g of methylene chloride, a white precipitate formed. The precipitate dissoved upon shaking and slowly recrystallized as white needles. There was no trimethylchlorosilane detected in the residual fluid, indicating that the expected reaction to form 1,1-diacetamidosilacyclobutane did not occur.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04985565 |
| 출처 데이터셋 | uspto-grants-1991_01 |
| ORD ID | ord-c2cd10faa21e40fbbb19209d3ea4c1b8 |
| 출처 메모 | uspto-grants-1991_01 |