1-Bromo-4-(trimethoxymethyl)benzene → HCID 15021999, 화합물

반응식

[OH:1][CH2:2][C:3]([CH2:9][OH:10])([CH2:6][CH2:7][CH3:8])[CH2:4][SH:5].CO[C:13](OC)(OC)[C:14]1[CH:19]=[CH:18][C:17]([Br:20])=[CH:16][CH:15]=1>>[Br:20][C:17]1[CH:18]=[CH:19][C:14]([C:13]23[S:5][CH2:4][C:3]([CH2:6][CH2:7][CH3:8])([CH2:9][O:10]2)[CH2:2][O:1]3)=[CH:15][CH:16]=1

참가 물질

반응물 2

HCID 135812791-Bromo-4-(trimethoxymethyl)benzene

HCID 15021997HCID 15021997, 화합물

생성물 1

HCID 15021999HCID 15021999, 화합물

실험 절차

(iv)b) Using a method analogous to that described in (iv)(a) above 2,2-di-(hydroxymethyl)-pentan-1-thiol and trimethyl 4-bromo-orthobenzoate were reacted together to give 1-(4-bromophenyl)-4-n-propyl-2,6-dioxa-7-thiabicyclo[2,2,2]octane.

후처리

customwere reacted together

출처 및 근거

ORD 기록: ord-ac173d9567ba42b48bd198acfdcdbf8c
출처 데이터셋: uspto-grants-1991_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04985582

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