5-Chloro-2-(methylthio)aniline → N-[5-chloro-2-(methylthio)phenyl]furan-2-sulfonamide

HRID 70414

반응식

HRID 70414 반응식
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([S:9][CH3:10])=[C:6]([NH2:8])[CH:7]=1.[O:11]1[CH:15]=[CH:14][CH:13]=[C:12]1[S:16](Cl)(=[O:18])=[O:17]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([S:9][CH3:10])=[C:6]([NH:8][S:16]([C:12]2[O:11][CH:15]=[CH:14][CH:13]=2)(=[O:18])=[O:17])[CH:7]=1

참가 물질

3

반응물 2

HCID 27945775-Chloro-2-(methylthio)anilineHCID 2795072Furan-2-sulfonyl Chloride

생성물 1

HCID 57378994N-[5-chloro-2-(methylthio)phenyl]furan-2-sulfonamide수율 47.2%

실험 절차

Following General Procedure B, the title compound (215 mg, 47%) was prepared from 5-chloro-2-methylsulfanyl-phenylamine (260 mg, 1.50 mmol) and furan-2-sulfonyl chloride (250 mg, 1.50 mmol).

출처 및 근거

ORD 기록
ord-5a58bf7e66f449a6be9727d840dfc16f
출처 데이터셋
uspto-grants-2014_09
특허 번호
US08822530B2

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