Potassium Carbonate → Methyl 2-(((2-amino-4-chlorophenyl)thio)methyl)benzoate
반응식
[NH2:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[SH:9].Br[CH2:11][C:12]1[CH:21]=[CH:20][CH:19]=[CH:18][C:13]=1[C:14]([O:16][CH3:17])=[O:15].C([O-])([O-])=O.[K+].[K+]>CN(C=O)C>[NH2:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[S:9][CH2:11][C:12]1[CH:21]=[CH:20][CH:19]=[CH:18][C:13]=1[C:14]([O:16][CH3:17])=[O:15]참가 물질
5
실험 절차
Following General Procedure A, the title compound (1.6 g, 84%) was prepared from 2-amino-4-chlorobenzenethiol (969 mg, 6.06 mmol), methyl 2-(bromomethyl)benzoate (1.4 g, 6.11 mmol) and K2CO3 (4.2 g, 30.55 mmol) in DMF (50 ml).
출처 및 근거
- ORD 기록
- ord-f14e56334d654acb98e80506c6ef5cc4
- 출처 데이터셋
- uspto-grants-2014_09
- 특허 번호
- US08822530B2
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