참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Diethylamine | HCID 8021 | — |
| 반응물 | Propanoyl chloride, 3-bromo- | HCID 84944 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 3-Bromo-n,n-diethylpropanamide | HCID 226112 | — |
반응 단계
A mixture of 3-bromopropanoyl chloride (1.0 g, 5.8 mmol) and diethylamine (1.9 g, 26 mmol) in THF (20 ml) was stirred at 0° C. for 30 min, the resulting white solid was filtered and the filtrate was concentrated to give a crude oil which was used in the next reaction without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08822530B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_09 |
|---|
| ORD ID | ord-bb963a68e9dd4b3f84fe5e6051568428 |
|---|
| 출처 메모 | uspto-grants-2014_09 |
|---|
