Ethyl isocyanate → HCID 44514481, 화합물

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[N:1]1([C:7]2[N:12]=[C:11]([N:13]3[CH2:18][CH2:17][O:16][CH2:15][CH2:14]3)[N:10]=[C:9]([C:19]3[CH:25]=[CH:24][C:22]([NH2:23])=[CH:21][CH:20]=3)[N:8]=2)[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[CH2:26]([N:28]=[C:29]=[O:30])[CH3:27]>>[N:1]1([C:7]2[N:12]=[C:11]([N:13]3[CH2:18][CH2:17][O:16][CH2:15][CH2:14]3)[N:10]=[C:9]([C:19]3[CH:25]=[CH:24][C:22]([NH:23][C:29]([NH:28][CH2:26][CH3:27])=[O:30])=[CH:21][CH:20]=3)[N:8]=2)[CH2:2][CH2:3][O:4][CH2:5][CH2:6]1

참가 물질

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HCID 8022Ethyl isocyanate

HCID 453790874-(4,6-Dimorpholino-1,3,5-triazin-2-yl)aniline

생성물 1

HCID 44514481HCID 44514481, 화합물

실험 절차

Starting from 4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)aniline (0.130 g 0.38 mmoles) and ethyl isocyanate (260 mg, 10 fold excess) the title compound was isolated as a white solid. Yield; 38 mg (25%); (M+H)=414.4

출처 및 근거

ORD 기록: ord-d69611bd945449e2829f1668221d0267
출처 데이터셋: uspto-grants-2015_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09174963B2

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