Propyl Acetate → HCID 22155088, 화합물

HRID 707743

반응식

HRID 707743 반응식
[C:1]([O:4][CH2:5][CH2:6][CH3:7])(=[O:3])[CH3:2]>C(O)C>[CH2:1]([OH:3])[CH3:2].[C:1]([O:4][CH2:5][CH2:6][CH3:7])(=[O:3])[CH3:2]

참가 물질

3

반응물 1

HCID 7997Propyl Acetate

생성물 1

HCID 22155088HCID 22155088, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

반응 조건

온도
60 °C

실험 절차

The dried high DS starch hexanoate described above (Ex. 12, 71.3 g), ethanol (65.2 g), and n-propyl acetate (65.2 g) were charged to a 500 mL round bottom flask, equipped with condenser, overhead stirrer, nitrogen blanket, thermocouple and heating mantle. The mixture was heated to 60° C. for about 1 hr. to form a transparent, low viscosity solution at 30 wt % solids in 50/50 ethanol/n-propyl acetate.

후처리

  1. additionwere charged to a 500 mL round bottom flask
  2. customequipped with condenser
  3. temperatureoverhead stirrer, nitrogen blanket, thermocouple and heating mantle

출처 및 근거

ORD 기록
ord-ba198b69b5fb4b6aaa592aab49863e33
출처 데이터셋
uspto-grants-2015_11
특허 번호
US09175179B2

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