Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalyl chloride → Dimethyl-1,3-oxazole-5-carbonyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | Dimethyl-1,3-oxazole-5-carboxylic acid | HCID 1132979 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Dimethyl-1,3-oxazole-5-carbonyl chloride | HCID 12336332 | — |
반응 단계
To a stirring solution of 2,4-dimethyl-oxazole-5-carboxylic acid (30 mg) in DCM (2.0 mL), oxalyl chloride (3.0 eq) was added at room temperature. The reaction mixture was stirred for 30 minutes. Solvents were evaporated and dried under vacuo to afford 2,4-dimethyl-oxazole-5-carbonyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09175003B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-051aa11aea3d49acb73551ed03209563 |
| 출처 메모 | uspto-grants-2015_11 |