5-[(2-Chlorobenzyl)sulfanyl]-2,3-dimethoxypyridine → 5-[(2-Chlorobenzyl)sulfanyl]-3-hydroxypyridin-2(1H)-one

HRID 709062노트

반응식

HRID 709062 반응식
C(SC1C=C(O)C(=O)NC=1)C1C=CC=CC=1.[Cl:17][C:18]1[CH:35]=[CH:34][CH:33]=[CH:32][C:19]=1[CH2:20][S:21][C:22]1[CH:23]=[C:24]([O:30]C)[C:25]([O:28]C)=[N:26][CH:27]=1>>[Cl:17][C:18]1[CH:35]=[CH:34][CH:33]=[CH:32][C:19]=1[CH2:20][S:21][C:22]1[CH:23]=[C:24]([OH:30])[C:25](=[O:28])[NH:26][CH:27]=1

참가 물질

3

반응물 2

HCID 711863175-[(2-Chlorobenzyl)sulfanyl]-2,3-dimethoxypyridine2회HCID 71187166HCID 71187166, 화합물

생성물 1

HCID 711859775-[(2-Chlorobenzyl)sulfanyl]-3-hydroxypyridin-2(1H)-one

실험 절차

Prepared as described for 5-(benzylsulfanyl)-3-hydroxypyridin-2(1H)-one (Example 1) from 5-[(2-chlorobenzyl)sulfanyl]-2,3-dimethoxypyridine (Intermediate 10).

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-56963d8dfd87422980dc4b8cd9820521
출처 데이터셋
uspto-grants-2015_11
특허 번호
US09180122B2

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