5-(4-Fluorobenzylthio)-2,3-dimethoxypyridine → 5-[(4-Fluorobenzyl)sulfanyl]-3-hydroxypyridin-2(1H)-one

HRID 709066노트

반응식

HRID 709066 반응식
C(SC1C=C(O)C(=O)NC=1)C1C=CC=CC=1.[F:17][C:18]1[CH:35]=[CH:34][C:21]([CH2:22][S:23][C:24]2[CH:25]=[C:26]([O:32]C)[C:27]([O:30]C)=[N:28][CH:29]=2)=[CH:20][CH:19]=1>>[F:17][C:18]1[CH:35]=[CH:34][C:21]([CH2:22][S:23][C:24]2[CH:25]=[C:26]([OH:32])[C:27](=[O:30])[NH:28][CH:29]=2)=[CH:20][CH:19]=1

참가 물질

3

반응물 2

HCID 711864345-(4-Fluorobenzylthio)-2,3-dimethoxypyridine2회HCID 71187166HCID 71187166, 화합물

생성물 1

HCID 711872155-[(4-Fluorobenzyl)sulfanyl]-3-hydroxypyridin-2(1H)-one

실험 절차

Prepared as described for 5-(benzylsulfanyl)-3-hydroxypyridin-2(1H)-one (Example 1) from 5-(4-fluorobenzylthio)-2,3-dimethoxypyridine (Intermediate 14).

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-8af1eda3feaa4490b8d25c28e66356ce
출처 데이터셋
uspto-grants-2015_11
특허 번호
US09180122B2

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