Triethylamine → HCID 178443076, 화합물

HRID 709328

반응식

HRID 709328 반응식
S(Cl)(Cl)=O.[NH:5]([C:10]([CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])=[O:11])[CH2:6][C:7]([OH:9])=O.[NH2:27][C@H:28]([C:35]([OH:37])=[O:36])[CH2:29][C:30]1[N:34]=[CH:33][NH:32][CH:31]=1.C(N(CC)CC)C>C1(C)C=CC=CC=1>[NH:5]([C:10]([CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])=[O:11])[CH2:6][C:7]([NH:27][C@H:28]([C:35]([OH:37])=[O:36])[CH2:29][C:30]1[N:34]=[CH:33][NH:32][CH:31]=1)=[O:9]

참가 물질

6

반응물 4

HCID 8471TriethylamineHCID 24386Thionyl ChlorideHCID 151008N-PalmitoylglycineHCID 178419078HCID 178419078, 화합물

생성물 1

HCID 178443076HCID 178443076, 화합물

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

Using thionyl chloride, N-palmitoyl-Gly was converted to the acid chloride in toluene at room temperature, then reacted with L-histidine using triethylamine as the base. However, only a trace amount of N-palmitoyl-Gly-His formed.

출처 및 근거

ORD 기록
ord-3b47184941904363ac92444c72623d0e
출처 데이터셋
uspto-grants-2015_11
특허 번호
US09180201B2

연결된 노트

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