Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Chloro-4-ethoxybenzaldehyde → 4-Butoxy-3-chlorobenzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Chloro-4-ethoxybenzaldehyde | HCID 4770035 | — |
| 반응물 | 4-Butoxy-3-chlorobenzaldehyde | HCID 54795206 | — |
| 생성물 | 4-Butoxy-3-chlorobenzoic acid | HCID 21105476 | 85% |
반응 단계
When the product of Step A was substituted for 3-chloro-4-ethoxybenzaldehyde in Example 49, Step A the identical process afforded the title compound in 85% yield. 1H-NMR (CDCl3) 0.96 (tr, 3H, J=7.38 Hz); 1.46-1.57 (m, 2H); 1.59-2.77 (m, 2H); 4.1 (tr, 2H, J=6.45 Hz); 6.93 (d, 1H, J=8.67 Hz); 7.96 (dd, 1H, J=8.64, 2.1 Hz); 8.1 (d, 1H, J=2.07 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09181182B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-78fbe9da51ab41688f41d4728e495fc5 |
| 출처 메모 | uspto-grants-2015_11 |