Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bromine → HCID 178516705, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bromine | HCID 24408 | — |
| 반응물 | HCID 178516710 | HCID 178516710 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | HCID 178516705 | HCID 178516705 | 90% |
반응 단계
Bromine (0.895 mL, 15.5 mmol) was added to the solution of quinoxalin-2-ol (1.5 g, 10.3 mmol) in HOAc (15 mL), the mixture was stirred at r.t. for 6 h, and the precipitate was collected and washed with ethyl ether and dried to afford 7-bromoquinoxalin-2-ol as a solid in 90% yield (2 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09181264B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-f19a51d543424f9b8ea1bc10a8a907b6 |
| 출처 메모 | uspto-grants-2015_11 |