참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | 7-Bromo-2-chloroquinoxaline | HCID 4913253 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 7-Bromo-2-hydrazinylquinoxaline | HCID 5200265 | 87% |
반응 단계
To the solution of 7-bromo-2-chloroquinoxaline (2 g, 8.2 mmol) in ethanol (20 mL) was added hydrazine hydrate (85%, 4.5 mL, 32.8 mmol). The mixture was heated to 78° C. for 2 h. After cooling to r.t., the precipitate was collected by filtration to afford 7-bromo-2-hydrazinylquinoxaline as white solid in 87% yield (1.7 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US09181264B2 |
|---|
| 출처 데이터셋 | uspto-grants-2015_11 |
|---|
| ORD ID | ord-08c8fad82e5d4612abccac1ebd254385 |
|---|
| 출처 메모 | uspto-grants-2015_11 |
|---|
