Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,9-Nonanediol → 2-(9-Hydroxynonyloxy)-6-nitrobenzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,9-Nonanediol | HCID 19835 | — |
| 반응물 | 1,1,3,3-Tetramethylguanidine | HCID 66460 | — |
| 반응물 | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| 반응물 | Dinitrobenzonitrile | HCID 520718 | — |
| 생성물 | 2-(9-Hydroxynonyloxy)-6-nitrobenzonitrile | HCID 66745844 | 30.7% |
반응 단계
Prepared as in Example 274c (except DBU was replaced with 1,1,3,3-tetramethylguanidine) from 1,9-nonanediol and 2,6-dinitrobenzonitrile in 30.7% yield. MS 307 (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09181276B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-cb45c08645774286b14ae0252469b5ee |
| 출처 메모 | uspto-grants-2015_11 |