Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methylmorpholine → N'-(3,3-dimethylbutanoyl)-4-nitrobenzohydrazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methylmorpholine | HCID 7972 | — |
| 반응물 | 3,3-Dimethylbutanoyl chloride | HCID 81514 | — |
| 반응물 | Benzoic acid, 4-nitro-, hydrazide | HCID 3693744 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | N'-(3,3-dimethylbutanoyl)-4-nitrobenzohydrazide | HCID 4628581 | — |
반응 단계
A suspension of 4-nitrobenzohydrazide (0.500 g, 2.76 mmol), and 4-methylmorpholine (0.455 ml, 4.14 mmol) were stirred in dichloromethane (20 ml). 3,3-Dimethylbutanoyl chloride (0.422 ml, 3.04 mmol) was added and the reaction mixture was stirred for 2 hours. Normal phase chromatography of the crude reaction mixture gave the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09187472B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-d3eefdfaafde46aa8c22e981e8c9e2e2 |
| 출처 메모 | uspto-grants-2015_11 |