Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → 1,1'-(cyclohexane-1,3-diylbis(methylene))bis(1H-pyrrole-2,5-dione)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Maleic Anhydride | HCID 7923 | — |
| 반응물 | 1,3-Bis(aminomethyl)cyclohexane | HCID 17406 | — |
| 반응물 | Sodium Acetate | HCID 517045 | — |
| 생성물 | 1,1'-(cyclohexane-1,3-diylbis(methylene))bis(1H-pyrrole-2,5-dione) | HCID 19078003 | — |
반응 단계
The general procedure was carried out using maleic anhydride (20.59 g, 210 mmol), 1,3-cyclohexanebis(methylamine) (14.22 g, 100 mmol), sodium acetate (1.64 g, 20 mmol), and acetic anhydride (22.46 g, 220 mmol). The resulting compound was purified by column chromatography (98:2 DCM:EtOAc), and the product obtained as a white solid (3.55 g/12%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09193139B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-b112c6558d17474381996a5ae79a3840 |
| 출처 메모 | uspto-grants-2015_11 |