1-Hexanesulfonyl chloride → Tert-butyl 3-(3-(hexylsulfonamido)phenyl)propylcarbamate

반응식

C1(C[NH:8][C:9]2[CH:10]=[C:11]([CH2:15][CH2:16][CH2:17][NH:18][C:19](=[O:25])[O:20][C:21]([CH3:24])([CH3:23])[CH3:22])[CH:12]=[CH:13][CH:14]=2)CCCCC1.[CH2:26]([S:32](Cl)(=[O:34])=[O:33])[CH2:27][CH2:28][CH2:29][CH2:30][CH3:31]>>[CH2:26]([S:32]([NH:8][C:9]1[CH:10]=[C:11]([CH2:15][CH2:16][CH2:17][NH:18][C:19](=[O:25])[O:20][C:21]([CH3:22])([CH3:23])[CH3:24])[CH:12]=[CH:13][CH:14]=1)(=[O:34])=[O:33])[CH2:27][CH2:28][CH2:29][CH2:30][CH3:31]

참가 물질

반응물 2

HCID 845041-Hexanesulfonyl chloride

HCID 59317002Tert-butyl 3-(3-(cyclohexylmethylamino)phenyl)propylcarbamate

생성물 1

HCID 68522737Tert-butyl 3-(3-(hexylsulfonamido)phenyl)propylcarbamate

실험 절차

Sulfonation of aniline 17 by hexane-1-sulfonyl chloride following the method used in Example 6 gives tert-butyl 3-(3-(hexylsulfonamido)phenyl)propylcarbamate.

출처 및 근거

ORD 기록: ord-d98234c7578d4b00a67646d1c9b96017
출처 데이터셋: uspto-grants-2015_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09193669B2

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