Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,4-Dimethyl-3-cyclohexene carboxaldehyde → HCID 86702760, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,4-Dimethyl-3-cyclohexene carboxaldehyde | HCID 93375 | — |
| 반응물 | Phenethyltriphenylphosphonium bromide | HCID 10863251 | — |
| 생성물 | HCID 86702760 | HCID 86702760 | 61.4% |
반응 단계
Starting from phenethyltriphenylphosphonium bromide (3.67 g, 8.20 mmol, 1.0 equiv.), n-Buli (1.6 M in hexanes, 5.1 mL, 8.20 mmol, 1.0 equiv.) and 2,4-dimethylcyclohex-3-enecarbaldehyde (1.70 g, 12.3 mmol, 1.5 equiv.), 1.14 g (61%) of the title compound as a colorless oil was obtained after purification by flash chromatography on SiO2 (cyclohexane).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09193935B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-fd3b54b74f0940d2840aa364e43a0061 |
| 출처 메모 | uspto-grants-2015_11 |