Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,1,3-Benzothiadiazole-4-carbaldehyde → (S)-N-(benzo[c][1,2,5]thiadiazol-4-ylmethyl)-1,1-diethoxypropan-2-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,1,3-Benzothiadiazole-4-carbaldehyde | HCID 2776283 | — |
| 반응물 | (2S)-1,1-Diethoxy-2-propanamine | HCID 12398111 | — |
| 생성물 | (S)-N-(benzo[c][1,2,5]thiadiazol-4-ylmethyl)-1,1-diethoxypropan-2-amine | HCID 67088326 | 95% |
반응 단계
According to the procedure described in the synthesis method of Compound IX-2, (S)-1,1-diethoxypropan-2-amine (Compound XIX-1) 883 mg (6.0 mmol) was reacted with benzo[c][1,2,5]thiadiazole-4-carbaldehyde 837 mg (5.1 mmol) to obtain the title compound 1.41 g (95%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09193734B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-f48c7a0f494e4973b3e5636258688ac0 |
| 출처 메모 | uspto-grants-2015_11 |