Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → 1-Methoxycarbonyl-2-isopropylidene hydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | Water | HCID 962 | — |
| 반응물 | Methyl carbazate | HCID 80519 | — |
| 생성물 | 1-Methoxycarbonyl-2-isopropylidene hydrazine | HCID 909521 | 89% |
반응 단계
Hydrazinecarboxylic acid methyl ester (5.01 g) were dissolved in acetone (28 mL), and acetic acid (0.0636 mL) was added. The reaction mixture was stirred at room temperature for 24 hours. Water (50 mL) was added, and mixture was extracted three times with DCM (50 mL) and evaporated under vacuum, giving N′-Isopropylidene-hydrazine-carboxylic acid methyl ester (6.45 g, 89%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08822430B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-925df8772b744ebba43c47590e0cb8bb |
| 출처 메모 | uspto-grants-2014_09 |