Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → HCID 22597223, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Acryloyl chloride | HCID 13140 | — |
| 반응물 | 2-Methyl-2-adamantanol | HCID 136545 | — |
| 생성물 | HCID 22597223 | HCID 22597223 | 55% |
반응 단계
200 mL of diethyl ether was put into a round-neck flask, 41.5 g of 2-methyl-2-adamantanol and 27.6 g of tetraethyl amine were added thereto and then 22.6 g of acryloyl chloride was dropped. The reactant was reacted at room temperature for about 12 hours and then filtered using diethyl ether. Subsequently, the solvent was removed by an evaporator and then the reactant product was obtained using vacuum distillation (yield: 55%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07084227B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-36f2de1457284bf3b0fda06e472eab7b |
| 출처 메모 | uspto-grants-2006_08 |