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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 7193생성일: 2026년 10월 24일

Diethyl Ether → HCID 22597223, 화합물

https://huagongshe.com/ko/reaction/7193

반응식

참여 물질

역할이름HCID투입량
반응물Diethyl EtherHCID 3283—
반응물Acryloyl chlorideHCID 13140—
반응물2-Methyl-2-adamantanolHCID 136545—
생성물HCID 22597223HCID 2259722355%

반응 단계

200 mL of diethyl ether was put into a round-neck flask, 41.5 g of 2-methyl-2-adamantanol and 27.6 g of tetraethyl amine were added thereto and then 22.6 g of acryloyl chloride was dropped. The reactant was reacted at room temperature for about 12 hours and then filtered using diethyl ether. Subsequently, the solvent was removed by an evaporator and then the reactant product was obtained using vacuum distillation (yield: 55%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07084227B2
출처 데이터셋uspto-grants-2006_08
ORD IDord-36f2de1457284bf3b0fda06e472eab7b
출처 메모uspto-grants-2006_08