Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-4-(3-nitrophenyl)thiazole → N-[4-(3-nitrophenyl)-1,3-thiazol-2-yl]-4-propylbenzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-4-(3-nitrophenyl)thiazole | HCID 613504 | — |
| 반응물 | 4-N-Propylbenzenesulphonyl chloride | HCID 2737222 | — |
| 생성물 | N-[4-(3-nitrophenyl)-1,3-thiazol-2-yl]-4-propylbenzenesulfonamide | HCID 10135798 | — |
반응 단계
The title compound was prepared from 2-amino-4-(3-nitrophenyl)thiazole and 4-n-propylbenzenesulfonyl chloride as described in the synthetic METHOD B to give a yellow solid (41.5 mg) with purity >90%: MS (pos) m/z 404.1, (neg) m/z 402.2; HRMS m/z 403.0062 (calc. of monoisotopic mass for Cl18H17N3O4S2 gives 403.0060).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07132436B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-b4b89f8535a04d2ab8c91439b7586ed6 |
| 출처 메모 | uspto-grants-2006_11 |