2,4,6-Trichlorobenzenesulfonyl chloride → HCID 10183010, 화합물

HRID 719345

반응식

HRID 719345 반응식
[Cl:1][C:2]1[CH:6]=[CH:5][S:4][C:3]=1[C:7]1[N:8]=[C:9]([NH2:12])[S:10][CH:11]=1.[Cl:13][C:14]1[CH:19]=[C:18]([Cl:20])[CH:17]=[C:16]([Cl:21])[C:15]=1[S:22](Cl)(=[O:24])=[O:23]>>[Cl:13][C:14]1[CH:19]=[C:18]([Cl:20])[CH:17]=[C:16]([Cl:21])[C:15]=1[S:22]([NH:12][C:9]1[S:10][CH:11]=[C:7]([C:3]2[S:4][CH:5]=[CH:6][C:2]=2[Cl:1])[N:8]=1)(=[O:24])=[O:23]

참가 물질

3

반응물 2

HCID 5213352,4,6-Trichlorobenzenesulfonyl chlorideHCID 14884414-(3-Chloro-2-thienyl)-1,3-thiazol-2-amine

생성물 1

HCID 10183010HCID 10183010, 화합물

실험 절차

The title compound was prepared from 4-(3-chloro-2-thienyl)-1,3-thiazol-2-amine and 2,4,6-trichlorobenzenesulfonyl chloride as described in the synthetic METHOD B to give a white solid (5.0 mg) with purity >90%. MS (pos) m/z 459.1, 461.1, 463.1.

출처 및 근거

ORD 기록
ord-28855e6d2af649ac9b55d25266f03852
출처 데이터셋
uspto-grants-2006_11
특허 번호
US07132436B2

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