5-Chlorovaleryl chloride → HCID 21886968, 화합물

반응식

[CH2:1]1[C:11]2=[C:12]3[C:7](=[CH:8][CH:9]=[CH:10]2)[CH2:6][CH2:5][CH2:4][N:3]3[C:2]1=[O:13].[Cl:14][CH2:15][CH2:16][CH2:17][CH2:18][C:19](Cl)=[O:20]>>[Cl:14][CH2:15][CH2:16][CH2:17][CH2:18][C:19]([C:9]1[CH:8]=[C:7]2[C:12]3=[C:11]([CH2:1][C:2](=[O:13])[N:3]3[CH2:4][CH2:5][CH2:6]2)[CH:10]=1)=[O:20]

참가 물질

반응물 2

HCID 740895-Chlorovaleryl chloride

HCID 149184935,6-dihydro-4H-pyrrolo[3,2,1-ij]quinolin-2(1H)-one

생성물 1

HCID 21886968HCID 21886968, 화합물수율 64.9%

실험 절차

Using 5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinolin-2(1H)-one (3.46 g) and 5-chlorovaleryl chloride (3.4 g) according to the same method as that of Reference Example 1, the title compound (3.78 g) was obtained as pale yellow crystals having a melting point of 89 to 90° C.

출처 및 근거

ORD 기록: ord-259d230615cd4a1fb1558ad1174802e6
출처 데이터셋: uspto-grants-2006_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07132547B2

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