Acetonitrile → HCID 21889441, 화합물

HRID 720213노트

반응식

HRID 720213 반응식
[CH:1]([C:4]1[C:9]([N+:10]([O-:12])=[O:11])=[C:8]([CH:13]([CH3:15])[CH3:14])[CH:7]=[C:6]([CH:16]([CH3:18])[CH3:17])[C:5]=1[S:19]([OH:22])(=[O:21])=[O:20])([CH3:3])[CH3:2].C(#N)C.[Ag:26]=O>CC(C)=O>[CH:1]([C:4]1[C:9]([N+:10]([O-:12])=[O:11])=[C:8]([CH:13]([CH3:14])[CH3:15])[CH:7]=[C:6]([CH:16]([CH3:18])[CH3:17])[C:5]=1[S:19]([O-:22])(=[O:21])=[O:20])([CH3:2])[CH3:3].[Ag+:26]

참가 물질

5

반응물 3

HCID 6342AcetonitrileHCID 92152Silver(II) oxideHCID 218894203-Nitro-2,4,6-tri(propan-2-yl)benzene-1-sulfonic acid

생성물 1

HCID 21889441HCID 21889441, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

Into a flask was charged 20 parts by 2,4,6-triisopropyl-3-nitrobenzenesulfonic acid, 80 parts of acetonitrile and 40 parts of acetone, and the mixture was stirred at room temperature for 16 hours. To this was added 7.46 parts of silver oxide and the mixture was stirred for 16 hours at room temperature. The resulting mixture was filtrated and concentrated to obtain 23.68 parts of silver 2,4,6-triisopropyl-3-nitrobenzenesulfonate.

후처리

  1. stirringthe mixture was stirred for 16 hours at room temperature
  2. filtrationThe resulting mixture was filtrated
  3. concentrationconcentrated

출처 및 근거

ORD 기록
ord-b6723cc8ef694f04952780b5ed70cd0d
출처 데이터셋
uspto-grants-2006_11
특허 번호
US07135268B2

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