3-Bromopyridine → HCID 21892701, 화합물

HRID 720472노트

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HRID 720472 반응식
Br[C:2]1[CH:3]=[N:4][CH:5]=[CH:6][CH:7]=1.[O:8]=[C:9]1[C@@H:16]2[C@@H:12]([CH2:13][N:14]([C:17]([O:19][C:20]([CH3:23])([CH3:22])[CH3:21])=[O:18])[CH2:15]2)[CH2:11][CH2:10]1>>[C:20]([O:19][C:17]([N:14]1[CH2:15][CH:16]2[C:9]([OH:8])([C:2]3[CH:3]=[N:4][CH:5]=[CH:6][CH:7]=3)[CH2:10][CH2:11][CH:12]2[CH2:13]1)=[O:18])([CH3:23])([CH3:21])[CH3:22]

참가 물질

3

반응물 2

HCID 122863-BromopyridineHCID 29948688rel-1,1-Dimethylethyl (3aR,6aS)-hexahydro-4-oxocyclopenta[c]pyrrole-2(1H)-carboxylate

생성물 1

HCID 21892701HCID 21892701, 화합물수율 27%

실험 절차

3-Bromopyridine (4.36 g, 27.6 mmol) and the product from Example 44A (2.07 g, 9.19 mmol) were processed as described in Example 1E to afford the title compound (0.743 g, 27%). MS (DCI/NH3) m/z 305 (M+H)+.

출처 및 근거

ORD 기록
ord-6caac7f76e4848cc80d8020d32b82c90
출처 데이터셋
uspto-grants-2006_11
특허 번호
US07135484B2

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