L-Phenylalanine → HCID 68631493, 화합물

HRID 72100

반응식

HRID 72100 반응식
[NH2:1][C@H:2]([C:10]([OH:12])=[O:11])[CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[C:13]([O:18]C(=O)CCC)(=O)[CH2:14][CH2:15][CH3:16]>>[C:13]([NH2:1])(=[O:18])[CH2:14][CH2:15][CH3:16].[NH2:1][C@H:2]([C:10]([OH:12])=[O:11])[CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

참가 물질

3

반응물 2

HCID 6140L-PhenylalanineHCID 7798Butyric anhydride

생성물 1

HCID 68631493HCID 68631493, 화합물

반응 조건

온도
100 °C

실험 절차

5 g of phenylalanine was added to 20 mL of butyric anhydride and the resulting mixture heated to about 100° C. for about 3 h. Excess butyric anhydride was then removed under reduced pressure to provide a solid residue that was recrystallized from ethanol to provide phenylalanine butyramide.

후처리

  1. customExcess butyric anhydride was then removed under reduced pressure
  2. customto provide a solid residue that
  3. customwas recrystallized from ethanol

출처 및 근거

ORD 기록
ord-3e84eb0ed57b475cbbdee34bf3c5aaeb
출처 데이터셋
uspto-grants-2014_09
특허 번호
US08828960B2

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