참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | Butyl bromide | HCID 8002 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | 3-Nitro-p-cresol | HCID 16271 | — |
| 용매 | tert-Butyl methyl ether | HCID 15413 | — |
| 생성물 | 4-Butoxy-1-methyl-2-nitrobenzene | HCID 68977201 | — |
반응 단계
A mixture of 4-methyl-3-nitrophenol (10.0 g), butyl bromide (9.4 g), sodium carbonate (6.9 g) and DMF (50 mL) was heated at 80° C. for 7 hours. The cooled reaction solution was diluted with MTBE and washed twice each with water and sodium hydroxide solution. The organic phase was dried and concentrated. The product with the molecular weight of 209.25 (C11H15NO3) was obtained in this way; MS (ESI): 210 (M+H+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08828991B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_09 |
|---|
| ORD ID | ord-b54f415575cc437c907cf99427af312b |
|---|
| 출처 메모 | uspto-grants-2014_09 |
|---|
