Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → Methyl 8-methyl-1,4-dioxaspiro[4.5]decane-8-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | Lithium diisopropylamide | HCID 2724682 | — |
| 반응물 | Methyl 1,4-dioxaspiro[4.5]decane-8-carboxylate | HCID 10845708 | — |
| 생성물 | Methyl 8-methyl-1,4-dioxaspiro[4.5]decane-8-carboxylate | HCID 22591390 | — |
반응 단계
According to the process described in the literature (JP83-118577), methyl 1,4-dioxaspiro [4.5]decan-8-carboxylate was reacted with methyl iodide in the presence of LDA (lithium diisopropylamide) to obtain methyl 8-methyl-1,4-dioxaspiro [4.5]decan-8-carboxylate (the compound (1) of the above figure).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07138397B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-afc59317940e481da20834cadb4f253c |
| 출처 메모 | uspto-grants-2006_11 |