Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → 1-(3-fluoro-4-nitrophenyl)-1H-1,2,4-triazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | 1,2,3-Triazine | HCID 123047 | — |
| 반응물 | (3-Fluoro-4-nitrophenyl)hydrazine | HCID 21883867 | — |
| 생성물 | 1-(3-fluoro-4-nitrophenyl)-1H-1,2,4-triazole | HCID 21883919 | — |
반응 단계
The mixture consisting of 2.5 g of 3-fluoro-4-nitrophenylhydrazine, 1.2 g of [1,2,3]triazine and 50 ml of ethanol was heated to reflux with stirring for 6 hours. After concentrating the reaction mixture under reduced pressure, the residue was worked up by column chromatography (solvent: 99:1 dichloromethane:methanol; silica gel).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07138414B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-cd957a3c7bf34e4a974ca1e5c6db13fd |
| 출처 메모 | uspto-grants-2006_11 |