Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chloro-4,5-difluorobenzoyl Isocyanate → HCID 178488186, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chloro-4,5-difluorobenzoyl Isocyanate | HCID 11557583 | — |
| 반응물 | HCID 178488184 | HCID 178488184 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | HCID 178488186 | HCID 178488186 | — |
반응 단계
The solution of equivalent amounts of 2-chloro-4,5-difluorobenzoyl isocyanate was added dropwise to the solution of 30 mg of 2-methoxy-4-(5-methyl-4H-[1,2,4]triazol-3-yl)phenylamine in 3 ml of acetonitrile and the mixture was stirred at room temperature for 30 minutes. The solid was then filtered off with suction, stirred with isopropanol and dried under reduced pressure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07138414B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-9d63ce9c4ae741549cc6f9bc5d723dc6 |
| 출처 메모 | uspto-grants-2006_11 |