Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(3-Methyl-5-(2-nitrophenyl)-4H-1,2,4-triazol-4-yl)benzoic acid → 2-(3-(2-Aminophenyl)-5-methyl-4H-1,2,4-triazol-4-yl)benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(3-Methyl-5-(2-nitrophenyl)-4H-1,2,4-triazol-4-yl)benzoic acid | HCID 21883887 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2-(3-(2-Aminophenyl)-5-methyl-4H-1,2,4-triazol-4-yl)benzoic acid | HCID 21883868 | — |
반응 단계
was prepared by hydrogenating 400 mg of 2-[3-methyl-5-(2-nitrophenyl)-[1,2,4]triazol-4-yl]benzoic acid in the presence of Pd/C in tetrahydrofuran and purified by stirring with dichloromethane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07138414B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-197ab0f37be24bf0b716e4cde269af23 |
| 출처 메모 | uspto-grants-2006_11 |