Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-(2-Nitrophenyl)-1,3,4-oxadiazol-2-amine → 5-(2-Aminophenyl)-1,3,4-oxadiazol-2-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-(2-Nitrophenyl)-1,3,4-oxadiazol-2-amine | HCID 712042 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 생성물 | 5-(2-Aminophenyl)-1,3,4-oxadiazol-2-amine | HCID 5093885 | — |
반응 단계
Hydrogen was introduced at atmospheric pressure into the solution of 350 mg of 5-(2-nitrophenyl)-[1,3,4]oxadiazol-2-ylamine until the theoretical amount had been taken up. After filtering off the catalyst with suction and concentrating the mixture under reduced pressure, the remaining oily residue was purified by column chromatography (solvent: 95:5 dichloromethane/methanol; silica gel).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07138414B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-d726a4112522467aa7270fe17a87f474 |
| 출처 메모 | uspto-grants-2006_11 |