Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Aminobenzoic Acid → 2-(3-Aminophenyl)-5-phenylbenzoxazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Aminobenzoic Acid | HCID 7419 | — |
| 반응물 | 2-Amino-4-phenylphenol | HCID 14562 | — |
| 생성물 | 2-(3-Aminophenyl)-5-phenylbenzoxazole | HCID 10469229 | — |
반응 단계
Prepared by the method of Example 1a), from 2-amino-4-phenylphenol (674 mg, 3.6 mmol) and 3-aminobenzoic acid (500 mg, 3.6 mmol) the subtitle compound was obtained, 84 mg (8%). 1H NMR (CDCl3) δ 7.97(bs, 1H), 7.70–7.57(m, 5H), 7.49(t, 1H), 7.45–7.35(m, 2H), 6.96(d, J=7.9 Hz, 1H). MS 287 m/z (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07138425B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-1874b2c2cc2440eca82c6db87907196b |
| 출처 메모 | uspto-grants-2006_11 |