Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-4-phenylphenol → 2-(3-Amino-4-methoxyphenyl)-5-phenylbenzoxazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-4-phenylphenol | HCID 14562 | — |
| 반응물 | 3-Amino-4-methoxybenzoic acid | HCID 17823 | — |
| 생성물 | 2-(3-Amino-4-methoxyphenyl)-5-phenylbenzoxazole | HCID 9973058 | — |
반응 단계
Prepared by the method of Example 1a), from 2-amino-4-phenylphenol (554 mg, 2.9 mmol) and 4-methoxy-3-aminobenzoic acid (500 mg, 2.9 mmol) the subtitle compound was obtained, 111 mg (10%). 1H NMR (CDCl3) δ 7.84(s, 1H), 7.72–7.38(m, 9H), 6.93(d, J=8.3 Hz, 1H), 3.96(s, 3H). MS 316 m/z (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07138425B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-467254f43e1b435e8e3272287a105dd2 |
| 출처 메모 | uspto-grants-2006_11 |