Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(4-Chloro-3-methylphenyl)boronic acid → 2-(3-Nitro-6-propylaminophenyl)-5-(3-methyl-4-chlorophenyl)benzoxazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (4-Chloro-3-methylphenyl)boronic acid | HCID 3786632 | — |
| 반응물 | 2-(5-bromo-1,3-benzoxazol-2-yl)-4-nitro-N-propylaniline | HCID 5303802 | — |
| 생성물 | 2-(3-Nitro-6-propylaminophenyl)-5-(3-methyl-4-chlorophenyl)benzoxazole | HCID 21884356 | — |
반응 단계
Prepared by the method of Example 15d), from 2-(3-nitro-6-propylaminophenyl)-5-bromobenzoxazole (400 mg, 1.59 mmol) and 3-methyl-4-chlorophenylboronic acid (271 mg, 1.59 mmol) the subtitle compound was obtained (230 mg, 34%). The product was used directly in the next step without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07138425B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-a97a2b3cda264dfe995f4eef17468da3 |
| 출처 메모 | uspto-grants-2006_11 |