Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Propanediamine → 4-Iodobiphenyl
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Propanediamine | HCID 428 | — |
| 반응물 | Sodium Iodide | HCID 5238 | — |
| 반응물 | 4-Bromobiphenyl | HCID 7101 | — |
| 용매 | 1-Pentanol | HCID 6276 | — |
| 생성물 | 4-Iodobiphenyl | HCID 15322 | — |
반응 단계
30 g of 4-bromobiphenyl is dissolved in 40 mL of n-pentanol. 2 equivalents of sodium iodide and 10 mole % of 1,3-propanediamine are added to the 4-bromobiphenyl solution. The reaction mixture is refluxed at 130° C. for sixteen (16) hours to produce 4-iodobiphenyl, as shown in reaction scheme (5).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07138555B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-e26975268c1443fcb894981069a57230 |
| 출처 메모 | uspto-grants-2006_11 |