5-Chlorovaleryl chloride → 9-(5-chloropentanoyl)-1,2,6,7-tetrahydropyrido[3,2,1-ij]quinolin-3(5H)-one

HRID 722915

반응식

HRID 722915 반응식
[CH2:1]1[C:10]2[C:5]3=[C:6]([CH2:11][CH2:12][C:13](=[O:14])[N:4]3[CH2:3][CH2:2]1)[CH:7]=[CH:8][CH:9]=2.[Cl:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20](Cl)=[O:21]>>[Cl:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]([C:8]1[CH:9]=[C:10]2[C:5]3=[C:6]([CH2:11][CH2:12][C:13](=[O:14])[N:4]3[CH2:3][CH2:2][CH2:1]2)[CH:7]=1)=[O:21]

참가 물질

3

반응물 2

HCID 740895-Chlorovaleryl chlorideHCID 136945641,2,6,7-tetrahydro-5H-pyrido[3,2,1-ij]quinolin-3-one

생성물 1

HCID 218872599-(5-chloropentanoyl)-1,2,6,7-tetrahydropyrido[3,2,1-ij]quinolin-3(5H)-one

실험 절차

Using 2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-5-one and 5-chlorovaleryl chloride according to the same method as that of Reference Example 1, the title compound (3.53 g) was obtained as colorless crystals having a melting point of 83–84° C.

출처 및 근거

ORD 기록
ord-6aafe6411be646cf932f45dd72fda6c8
출처 데이터셋
uspto-grants-2006_11
특허 번호
US07138533B2

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