참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | (Chlorothio)formyl chloride | HCID 75990 | — |
| 반응물 | 4-Benzyloxybenzamide | HCID 2726431 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 5-(4-Benzyloxyphenyl)-[1,3,4]oxathiazol-2-one | HCID 59549525 | — |
반응 단계
4-benzyloxybenzamide (0.66 g, 2.98 mmol) and 0.26 ml of chlorocarbonyl sulfenyl chloride were dissolved in 10 ml of benzene, refluxed for 3 hours, and stirred at 50° C. for 12 hours. The organic solvent was distilled off under reduced pressure, and the resulting solid was washed with n-hexane to obtain 0.78 g of 5-(4-benzyloxy-phenyl)-[1,3,4]oxathiazol-2-one.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08828992B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_09 |
|---|
| ORD ID | ord-fbc85fb8b0574939b8b9d725112b0166 |
|---|
| 출처 메모 | uspto-grants-2014_09 |
|---|
