Benzaldehyde → HCID 67136987, 화합물
반응식
[O:1]([C:8]1[CH:13]=[CH:12][C:11]([NH:14][NH2:15])=[CH:10][CH:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:16](=O)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>CO>[CH:16](=[N:15][NH:14][C:11]1[CH:12]=[CH:13][C:8]([O:1][C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=2)=[CH:9][CH:10]=1)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1참가 물질
4
실험 절차
A suspension of (4-phenoxyphenyl)hydrazine (J. Org. Chem. 1956, 395; 1.5 g) in methanol (10 mL) was mixed with benzaldehyde (0.76 mL) and heated to reflux. The crystals which separated out on cooling were filtered off with suction. The product with the molecular weight of 288.35 (C19H16N2O); MS (ESI): 289 ([M+H]+), was obtained in this way.
후처리
- temperatureheated to reflux
- customThe crystals which separated out
- temperatureon cooling
- filtrationwere filtered off with suction
- customMS (ESI): 289 ([M+H]+), was obtained in this way
출처 및 근거
- ORD 기록
- ord-559485146324438eaa0a475c3a734b00
- 출처 데이터셋
- uspto-grants-2006_11
- 특허 번호
- US07141561B2
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