2,1,3-Benzothiadiazol-5-ylmethanol → 2,1,3-Benzothiadiazole-5-carbaldehyde

HRID 723518

반응식

HRID 723518 반응식
[N:1]1[S:5][N:4]=[C:3]2[CH:6]=[C:7]([CH2:10][OH:11])[CH:8]=[CH:9][C:2]=12>ClCCl.[O-2].[O-2].[Mn+4]>[N:1]1[S:5][N:4]=[C:3]2[CH:6]=[C:7]([CH:10]=[O:11])[CH:8]=[CH:9][C:2]=12

참가 물질

4

반응물 1

HCID 27762942,1,3-Benzothiadiazol-5-ylmethanol

생성물 1

HCID 27762902,1,3-Benzothiadiazole-5-carbaldehyde

시약·촉매·용매 2

HCID 178418406HCID 178418406, 화합물촉매HCID 6344Dichloromethane용매

실험 절차

This was prepared by oxidation of benzo[1,2,5]thiadiazol-5-yl-methanol (2a) with manganese dioxide in dichloromethane by the method of Example (4c).

출처 및 근거

ORD 기록
ord-c24eaf83cafd42cebb258a0d8ec55660
출처 데이터셋
uspto-grants-2006_11
특허 번호
US07141564B2

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