(1,2,3-Benzothiadiazol-5-yl)methanol → 1,2,3-Benzothiadiazole-5-carbaldehyde

HRID 723519

반응식

HRID 723519 반응식
[S:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][OH:11])=[CH:9][C:4]=2[N:3]=[N:2]1>ClCCl.[O-2].[O-2].[Mn+4]>[S:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH:10]=[O:11])=[CH:9][C:4]=2[N:3]=[N:2]1

참가 물질

4

반응물 1

HCID 21873619(1,2,3-Benzothiadiazol-5-yl)methanol

생성물 1

HCID 185046971,2,3-Benzothiadiazole-5-carbaldehyde

시약·촉매·용매 2

HCID 178418406HCID 178418406, 화합물촉매HCID 6344Dichloromethane용매

실험 절차

This was prepared by oxidation of benzo[1,2,3]thiadiazol-5-yl-methanol (6a) with manganese dioxide in dichloromethane by the method of Example (4c).

출처 및 근거

ORD 기록
ord-52575eded24940759c6cbef2c20f27d5
출처 데이터셋
uspto-grants-2006_11
특허 번호
US07141564B2

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