Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aniline → 4-Nitrodiphenylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | 1-Chloro-4-nitrobenzene | HCID 7474 | — |
| 반응물 | Formanilide | HCID 7671 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 용매 | Formic Acid | HCID 284 | — |
| 생성물 | 4-Nitrodiphenylamine | HCID 13271 | — |
반응 단계
formanilide method, where formic acid and aniline are used as starting materials to prepare formanilide, which in turn reacts with p-nitro-chlorobenzene in the presence of an acid-binding agent such as potassium carbonate, to produce 4-nitrodiphenylamine, and then, 4-nitrodiphenylamine is reduced by sodium sulfide to form 4-aminodiphenylamine;
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07084302B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-7a9eeef338d34ed09b7439bf73611b0e |
| 출처 메모 | uspto-grants-2006_08 |